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Lecturer(s)
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Course content
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The importance of analytical chemistry in the control of environmental pollution. Sources and behavior of pollutants in the environment. Sampling, quality assurance, preservation, transportation and storage of samples. Modification of the sample before analysis, extraction of solid and liquid samples Chromatographic methods and their use, data interpretation. Spectral methods and their use, data interpretation. Procedures for the determination of selected pollutant groups. Options for in-situ determination. Fundamentals of QA / QC. Calibration and method sensitivity, accuracy and accuracy of data, reproducibility and repeatability. Reference materials, enriched and blank samples,regulation diagrams. Fundamentals of GLP, method validation, interlaboratory comparative tests, accreditation.
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Learning activities and teaching methods
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- Contact hours
- 39 hours per semester
- Preparation for an examination (30-60)
- 60 hours per semester
- Preparation for laboratory testing; outcome analysis (1-8)
- 8 hours per semester
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| prerequisite |
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| Knowledge |
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| to calculate the amount of substance, the concentration, the composition of the solution |
| Calculate the amounts of reactants from the chemical equation |
| Describe basic principles of instrumental methods |
| describe the sampling procedure |
| Skills |
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| to work with charts |
| interpret the data obtained during the measurement |
| to assess the suitability of the analytical method for the planned measurement |
| learning outcomes |
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| Knowledge |
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| Name the basic groups of pollutants |
| Describe methods for extracting the analyte |
| Explain the principles of QA / QC |
| Explain GLP principles |
| Skills |
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| create a calibration dependency data, and use its equation to determine the content of the analyte |
| Design a procedure for sampling and sample processing with respect to analyte concentrations |
| Assess the suitability of different chromatographic methods |
| Assess the suitability of applying different types of spectral methods |
| teaching methods |
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| Knowledge |
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| Interactive lecture |
| Practicum |
| assessment methods |
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| Combined exam |
| Skills demonstration during practicum |
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Recommended literature
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Barek, Jiří; Opekar, František,; Štulík, Karel. Elektroanalytická chemie. 1. vyd. Praha : Karolinum, 2005. ISBN 80-246-1146-5.
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Miloslav Suchánek. KVALIMETRIE 16 Statistické metody v metrologii a analytické chemii. EURACHEM-ČR, 2009. ISBN 80-86322-04-1.
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Němcová Irena; Engst Pavel; Jelínek Ivan; Sejbal Jan; Rychlovský Petr. Spektrometrické analytické metody II. Praha, 1998. ISBN 80-7184-586-8.
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Němcová, Irena; Rychlovský, Petr; Čermáková, Ludmila. Spektrometrické analytické metody I. 2. vyd. Praha : Karolinum, 2004. ISBN 80-246-0776-X.
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OECD. Good Laboratory Practice: OECD Principles and Guidance for Compliance Monitoring. 2005. ISBN 9789264012837.
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Popl, Milan; Fähnrich, Jan. Analytická chemie životního prostředí. Vyd. 4., přeprac. Praha : Vydavatelství VŠCHT, 1999. ISBN 80-7080-336-3.
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Štulík, Karel. Analytické separační metody. 1. vyd. Praha : Karolinum, 2004. ISBN 80-246-0852-9.
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