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Course info
KET / MMA
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Course description
Department/Unit / Abbreviation
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KET
/
MMA
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Academic Year
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2024/2025
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Academic Year
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2024/2025
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Title
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Materials analysis methods for el. eng.
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Form of course completion
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Exam
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Form of course completion
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Exam
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Long Title
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Materials analysis methods for electrical engineering
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Accredited / Credits
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Yes,
5
Cred.
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Type of completion
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Combined
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Type of completion
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Combined
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Time requirements
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Lecture
2
[Hours/Week]
Tutorial
2
[Hours/Week]
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Course credit prior to examination
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Yes
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Course credit prior to examination
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Yes
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Automatic acceptance of credit before examination
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No
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Included in study average
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YES
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Language of instruction
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Czech, English
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Occ/max
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|
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Automatic acceptance of credit before examination
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No
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Summer semester
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0 / -
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0 / -
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0 / -
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Included in study average
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YES
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Winter semester
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12 / -
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0 / -
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0 / -
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Repeated registration
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NO
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Repeated registration
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NO
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Timetable
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Yes
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Semester taught
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Winter semester
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Semester taught
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Winter semester
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Minimum (B + C) students
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10
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Optional course |
Yes
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Optional course
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Yes
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Language of instruction
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Czech, English
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Internship duration
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0
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No. of hours of on-premise lessons |
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Evaluation scale |
1|2|3|4 |
Periodicity |
každý rok
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Evaluation scale for credit before examination |
S|N |
Periodicita upřesnění |
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Fundamental theoretical course |
Yes
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Fundamental course |
No
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Fundamental theoretical course |
Yes
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Evaluation scale |
1|2|3|4 |
Evaluation scale for credit before examination |
S|N |
Substituted course
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None
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Preclusive courses
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N/A
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Prerequisite courses
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N/A
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Informally recommended courses
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N/A
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Courses depending on this Course
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KET/SNTME
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Histogram of students' grades over the years:
Graphic PNG
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XLS
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Course objectives:
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The subject is focused on a comprehensive description of the various methods used to analyse physicochemical properties of materials for electrical engineering. Students will be acquainted with the relationship between the structure of substances and their physicochemical properties and with the theoretical principles of methods used for analysis of material properties. The course deals with the classification of methods, their basic principles and the design of measuring apparatuses. The emphasis is on the description of separation techniques (GC, GPC ...), spectrometric techniques (IR, FT-IR, BDS) as well as thermal analyses (DTA, DSC, TG, DTG, TMA, DMA). The described methods are supplemented with practical examples of their application during lectures and exercises.
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Requirements on student
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Credit recognition: attendance at the seminars and acceptation of seminar works by tutorial lecturer is required.
The examination comprises written and oral part.
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Content
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1. General aspects of the use of methods of material analysis in electrical engineering
2. Relation of structure and physicochemical properties of substances
3. Overview of methods and measured parameters for determination of properties of substances
4. Basic concepts and classification of structural analyses
5. Differential thermal analysis and differential scanning calorimetry (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice)
6. Thermogravimetry and Derivative Thermogravimetry (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice)
7. Dilatometry and thermomechanical analysis (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice)
8. Rheology and dynamic mechanical analysis (basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice, TTS diagrams)
9. Utilization of thermal analyses in the study of kinetics of chemical reactions
10. Separation techniques - basic principles, overview of measuring techniques, design of measuring apparatuses, examples of use in practice
11. Infrared spectroscopy - basic principles, overview of measuring techniques, design of IR spectrometers
12. Infrared spectroscopy - qualitative and quantitative methods of analysis, examples of the use of IR spectroscopy techniques in practice
13. Broadband dielectric spectroscopy and other special techniques of material analysis and their use
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Activities
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Fields of study
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Guarantors and lecturers
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-
Guarantors:
Prof. Ing. Radek Polanský, Ph.D. ,
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Lecturer:
Ing. Petr Kadlec, Ph.D. (60%),
Prof. Ing. Radek Polanský, Ph.D. (20%),
Ing. Pavel Prosr, Ph.D. (20%),
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Tutorial lecturer:
Ing. Petr Kadlec, Ph.D. (50%),
Prof. Ing. Radek Polanský, Ph.D. (100%),
Ing. Pavel Prosr, Ph.D. (50%),
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Literature
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Basic:
Mentlík, Václav. Diagnostika elektrických zařízení. Praha : BEN - technická literatura, 2008. ISBN 978-80-7300-232-9.
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Recommended:
Griffiths, Peter R.; De Haseth, James A. Fourier transform infrared spectrometry. 2nd ed. Hoboken : Wiley-Interscience, 2007. ISBN 978-0-471-19404-0.
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Recommended:
Crompton, T. R. Physical testing of plastics. Shrewsbury : Smithers Rapra Technology, 2012. ISBN 978-1-84735-485-3.
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Recommended:
Askeland, Donald R.; Fulay, Pradeep P.,; Wright, Wendelin J. The science and engineering of materials. 6th ed. Stamford : Cengage Learning, 2011. ISBN 978-0-495-29602-7.
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Recommended:
Wunderlich, Bernhard. Thermal analysis of polymeric materials. Berlin : Springer, 2005. ISBN 978-3-540-23629-0.
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On-line library catalogues
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Time requirements
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Full-time form of study
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Activities
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Time requirements for activity [h]
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Contact hours
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26
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Practical training (number of hours)
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26
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Graduate study programme term essay (40-50)
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45
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Preparation for an examination (30-60)
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45
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Preparation for laboratory testing; outcome analysis (1-8)
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8
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Total
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150
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Prerequisites
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Knowledge - students are expected to possess the following knowledge before the course commences to finish it successfully: |
no particular prerequisites are specified |
Skills - students are expected to possess the following skills before the course commences to finish it successfully: |
no particular prerequisites are specified |
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Learning outcomes
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Knowledge - knowledge resulting from the course: |
clarify the basic relationships between the structure and the physicochemical properties of the substances |
known the basic classification of methods and corresponding material properties used for physicochemical analysis of materials |
explain the basic principles of methods of material analysis of materials used in electrical engineering |
describe the design of the measuring instruments used for the material analysis |
evaluate on a particular example the advantages and disadvantages of applying a particular method |
Skills - skills resulting from the course: |
uses practically differential scanning calorimetry, thermogravimetry, thermomechanical analysis, dynamic mechanical analysis, Fourier transform infrared spectroscopy and broadband dielectric spectroscopy |
measures the material properties corresponding to the method |
finds appropriate professional literature |
evaluate the measured data on the basis of its own experience and with the help of specialized literature |
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Assessment methods
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Knowledge - knowledge achieved by taking this course are verified by the following means: |
Combined exam |
Skills - skills achieved by taking this course are verified by the following means: |
Skills demonstration during practicum |
Individual presentation at a seminar |
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Teaching methods
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Knowledge - the following training methods are used to achieve the required knowledge: |
Lecture supplemented with a discussion |
Multimedia supported teaching |
Self-study of literature |
Skills - the following training methods are used to achieve the required skills: |
Laboratory work |
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